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For a successful test of the elements of water Hofmann apparaturus für more than 5 mL electrolyte are needed. The following appliances were developed in a brain storming during a SINUS workshop. Another apparatus developed by Obendrauf consists of two syringes with paper clip electrodes.
Material:
2 Liquemin bottles full of sodium sulfate solution,
small plastic honey packing, 2 sterile hypodermic needles extracted
from an 1-mL insulin syringe, 9-Volt battery, electric wire with crocodile
clips, plastic pipette, goggles, candle, matches.
Experiment:
1. Pierce a small plastic
honey packing with two hypodermic needles extracted from an insulin
syringe.
Choose
a distance between the needles to have space for two bottles to be put
over them.
2. Cover the bottom of the
packing with sodium sulfate solution.
3. Make an electric connection
between the battery an the lower ends of the needles.
4. Carefully turn the bottles
full of sodium sulfate solution and put each of them over one of the needles.
5. Wait until the bottle
connected with the negative terminal of the battery is full of gas.
6. Ask your teacher to demonstrate
a test for pure hydrogen ("negative oxyhydrogen test").
7. In the other bottle a
test for pure oxygen is made ("glowing paper test").
Models
of smallest particles in air, hydrogen, oxygen, water.
THIS ANALYSIS WITH AN ACID BASE INDICATOR